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Text File  |  1991-12-13  |  3.8 KB  |  203 lines
  1. This liquid was soluble only in concentrated sulfuric acid.
  2. 1348
  3. Typical of neutral, oxygen-containing compounds.
  4. Solvent is deuterochloroform.
  5. ΦττΦΦΦΦΦΦΦτττΦΦΦΦττµµΦΦΦτµµµτττµττττµµΦΦΦττµττµσµµττµσΣµµµτττΦΦτττµµσσµτττττττττµµµττττµµσσσσµτττττττµµττττσµµτµµσσµτττµµµµττµµµµτττττµσµµµτττµµµτµµµµµµµττµµτττµµµµµµµµτΦτµµτµµµµµµµσµττττµσσµµµµµµµτµµσµτµτττµµµµσσπß▀▌┘╥╨═╩╦╬╧╤╘╪┌▌▀ΓΣσσµµµµµµµµµµµµµµµσµτΦτ
  6. µτΦΦµµµττττσσσµµµµµµσσσµτττττσσµτµµµµµµµµµµµµσσσµµµµµµσΣµµµµµµσµµµµµµµµµµµµµµµµµµµµσσσµµµµσσσµµµσσσσσσσσµσσµµµΣµµµµµµµµτµµσσµσσµµµσµµµµµσπΣΣΣσσσΣσσσσσσΣΣσσσσσσσσµσσπππππππππππππσµσσσΣΣσµσΣππßα▀ßßßßΓπππΓαα▀▀█╪╒╨╠┼┐╖░¼ªó¥¥ƒÑ½«░▓╡║┴├├──ñvS "*SS^t~åÆÿ₧Ѽ┤╜╞╬╤
  7. ╙╒┘█▌▐▐▐▐▐▄██▀αßΓππππππππππππΓα▀▐▀αßΓππππΣσσσπππΣΣσµµΣΓΓΓΓΣσΣΣπΣσµσπΣΣσµµµµσΣΣσσσσσσµµµσσΣΣµµµµµσΣπß▌┘╘╧╦▀ΓπΣΣσσΣππΦi┼!╝ÿ$├ '
  8.  
  9. 132023303334383941424344454648495154
  10. There is a ratio of 1 alkene proton to 11 aliphatic ones.
  11. Molecular ion is at 96.
  12. QΦCàD~`v7t'V6Q5F)HM.R._.a&
  13. 26
  14. The base peak (at 81) represents a loss of methyl from the molecular ion.
  15. The compound is UV transparent.
  16. #
  17. The unknown is not conjugated.
  18. No extra elements were detected.
  19. 212531353941424349264048
  20. The compound does not contain halides, nitrogen or sulfur.
  21. The liquid burnt with a clear flame leaving no residue.
  22. #
  23. This indicates a high hydrogen to carbon ratio.
  24. Below room temperature.
  25. #
  26. Typical for a liquid.
  27. Liquid film.
  28. #""""""!!!! !!!! !  !!!!!!      !!!!!#%&&''''*+,,,,-,,,,,,,,,,+++***(''(''''''''(()*++.6ENLQ_wwiâÜ╣╚µΦα▐╒╠╚╚╧╔╕åJ?;40/263/.-0683/*(((&&&%$%&%$$$######""""!!!""!!!!! !"""""""!"""!!  !!"!"!!!!!!!"""""""##%#"!!!!!!""""""!"""#"!! !!!!!"""!!!"!!!""##%&'&&&)+05
  29. -+++)&%%%&'&&&&&&&&'%%$$$%%&''''(*,/27ETg|êûíñºÇ^>:88<=>?@@;89=A=;866:>1.,-1?E2/.-0,*))))**+,-2117?PBJQj40///18=HY?7314;7437BJ941132/-/16F;320013=Le`:8BP>2.-.7<1--/19H<BZttL-*+1CH0+))(''D%$"$$%&&&%%%%&'(+18,'%%%%%#%$$$$$##$###$%(.(%''&%"#%2B02@-)++,- 
  30. 1419222427294231531320233033343839414243444546484951542850
  31. The compound is an unsaturated hydrocarbon (alkene).
  32. 108 to 110 degrees.
  33. #
  34. A typical value for a liquid.
  35. Optically inactive.
  36. #
  37. The compound is achiral.
  38. 0.810
  39. #
  40. Typical value for an organic liquid.
  41. 1.450
  42. #
  43. A typical value.
  44. #
  45. #
  46. #
  47. #
  48. #
  49. #
  50. Solvent is deuterochloroform.
  51. ª:sÖLd>gt:½t8╢t7ƒq6ìt
  52. 14192224272942
  53. Signals are from a tri-substituted alkene, 4 methylenes, 1 methyl.
  54. #
  55. #
  56. #
  57. #
  58. #
  59. #
  60. #
  61. #
  62. #
  63. No precipitate was formed.
  64. 2227282950
  65. This indicates that no aldehyde or ketone is present.
  66. No positive result.
  67. 3344454651
  68. The unknown contains no active hydrogens ie no OH, NH, or SH.
  69. #
  70. #
  71. #
  72. #
  73. #
  74. #
  75. #
  76. #
  77. #
  78. No reaction occurred.
  79. 14
  80. This compound is not an ester.
  81. #
  82. #
  83. #
  84. #
  85. #
  86. #
  87. #
  88. #
  89. #
  90. #
  91. #
  92. #
  93. #
  94. #
  95. #
  96. No positive result.
  97. 3344454651
  98. The unknown contains no NH or OH.
  99. #
  100. #
  101. #
  102. Reaction! The reagent's colour was discharged.
  103. #
  104. This indicates unsaturation.
  105. #
  106. #
  107. #
  108. No colour change was observed.
  109. 232850
  110. The compound is not a sugar.
  111. #
  112. #
  113. #
  114. A reaction was seen.
  115. #
  116. This indicates a reaction typical of a phenol or an alkene.
  117. No positive result.
  118. #
  119. This compound is not an ether.
  120. No change was noticed.
  121. #
  122. The unknown is not a phenol or an enol.
  123. #
  124. #
  125. #
  126. #
  127. #
  128. #
  129. #
  130. #
  131. #
  132. #
  133. #
  134. #
  135. #
  136. #
  137. #
  138. #
  139. #
  140. #
  141. #
  142. #
  143. #
  144. #
  145. #
  146. #
  147. A solution was obtained.
  148. #
  149. Typical of unsaturated or aromatic hydrocarbons.
  150. #
  151. #
  152. #
  153. #
  154. #
  155. #
  156. #
  157. #
  158. #
  159. #
  160. #
  161. #
  162. A reaction was observed.
  163. #
  164. The unknown compound could be unsaturated or a phenol.
  165. No change could be seen.
  166. #
  167. The compound is not an acetal, ester, amide, anhydride or nitrile etc.
  168. No positive result.
  169. 3344454651
  170. The compound contains no OH or NH groups.
  171. #
  172. #
  173. #
  174. #
  175. #
  176. #
  177. #
  178. #
  179. #
  180. #
  181. #
  182. #
  183. #
  184. #
  185. #
  186. #
  187. #
  188. #
  189. colourless liquid
  190. 010509
  191. 323652
  192. 0
  193. 2
  194. ç¥│╡┤░y¼╡vç╢½⌐╢╩b│«
  195. ç¥│╡┤░y¼ƒNq¡╡ñ╜┴e¬┴_óÑ
  196. liquid unsaturated hydrocarbon
  197. 5
  198. isomers of dimethylhexene
  199. 3,3-dimethyl-2-ethyl-1-butene
  200. 1-methylcyclohexene
  201. 3-ethyl-1-hexene
  202. 3-methyl-1-heptene
  203.